Pressurized Basic Electrochemical Cell - 10 bar, 50 mL

This pressurized electrochemical cell is designed for controlled laboratory experiments under elevated pressure conditions. With a total internal volume of 50 mL and a maximum operating pressure of 10 bar, it provides a robust and versatile platform for electrochemical studies. The cell features a chemically resistant PEEK chamber and lid, sealed with an O-ring and secured with two metal clamps, ensuring reliable, leak-tight operation. It is equipped with inlet and outlet ports for fluid or gas handling, as well as a dedicated port for a temperature probe. When a probe is not used, the port can be securely sealed with a plug. The cell supports both 2-electrode and 3-electrode configurations, offering flexibility for a wide range of electrochemical measurements. While the example configuration shown in pictures accommodates a plate-type working electrode using a sample holder, the design is also compatible with disk electrodes. All connections are based on Swagelok PFA fittings, some of which are modified with precision-drilled through-holes to allow for the integration of electrodes and a temperature probe. Please note electrodes are not included and must be selected separately (see compatible options below). This cell is not intended for hydrothermal reactions. Pressure should be supplied externally using a compressed gas system. Customization options, including alternative materials and design modifications, are available upon request. Application note This pressurized electrochemical cell is designed for a wide range of laboratory-scale experiments where controlled pressure conditions are required. Typical applications include: 1. Gas-involving electrochemical reactions - studies with gases such as CO₂, H₂, O₂, or N₂ under controlled pressure conditions. 2. Electrocatalysis research - evaluation of catalyst performance, activity, and stability in 2- and 3-electrode configurations. 3. CO₂ reduction (CO₂RR) and hydrogen evolution (HER) - experiments requiring enhanced gas solubility and controlled mass transport. 4. Electrochemical sensing and method development - development and validation of electroanalytical techniques under pressurized environments. 5. Battery and redox chemistry studies - investigation of liquid-phase electrochemical systems and redox-active materials. 6. Fundamental electrochemistry under pressure - research on pressure effects on reaction kinetics, transport phenomena, and electrode processes. 7. Material screening and compatibility testing - evaluation of electrode materials, membranes, and electrolytes in controlled environments. Specification maximum operating pressure: 10 bar total volume: 50 mL recommended volume of liquid: 30 - 35 mL maximum operating temperature: 200 ⁰C port for temperature probe: 1/8 in. (3.175 mm) electrode port diameter: 6 mm (1/4 in. possible on request) number of electrode ports: 3 recommended tubing: 1/8 in. OD PEEK tube Intrastat data HS Code: 90309000 Country of Origin: Sweden NET weight: 700g Safety note The use of a High-Pressure Electrochemical Cell involves working with equipment capable of withstanding elevated pressures and conducting experiments with potentially reactive chemicals. Ensuring safety during operation is paramount to prevent accidents and protect personnel and equipment. Below are key safety considerations to observe when using the High-Pressure Electrochemical Cell: 1. Prior to operation, all personnel involved should receive comprehensive training on the setup, operation, and safety protocols associated with the High-Pressure Electrochemical Cell. Only trained individuals familiar with the equipment should be permitted to operate it. 2. Adhere strictly to the specified pressure limitations of the High-Pressure Electrochemical Cell. Do not exceed the recommended pressure range to prevent over-pressurization, which could lead to equipment failure and potential hazards. 3. Ensure that all materials, including electrodes, seals, and electrolytes, are compatible with the pressure and chemical environment inside the cell. Incompatibilities could result in leaks, corrosion, or other safety hazards. 4. Verify that the pressure relief mechanism is in place and functioning correctly. This mechanism is crucial for safely releasing excess pressure in the event of over-pressurization. 5. Regularly inspect the seals and connections of the High-Pressure Electrochemical Cell for signs of wear, damage, or leaks. Replace any compromised components promptly to maintain sealing integrity and prevent pressure-related accidents. 6. Establish clear emergency procedures, including evacuation routes and protocols for handling pressure-related incidents. Ensure that all personnel are aware of these procedures and know how to respond effectively in case of emergencies. 7. Wear appropriate Personal Protective Equipment (PPE), including safety glasses, gloves, and lab coats, when operating the High Pressure Electrochemical Cell. Additional PPE may be necessary depending on the specific experimental conditions and hazards involved. 8. Supervise experiments closely and monitor the High-Pressure Electrochemical Cell continuously during operation. Respond promptly to any abnormalities or unexpected changes in pressure or performance. By adhering to these safety guidelines and exercising caution and diligence, users can minimize risks and ensure the safe and effective operation of the High-Pressure Electrochemical Cell in the laboratory. Always prioritize safety to protect yourself, your colleagues, and the integrity of the experimental setup. Product includes 1 x PEEK chamber 1 x PEEK lid 2 x Stainless Steel 316L clamp 1 x set of Stainless Steel screws 3 x electrode fitting, modified Swagelok PFA 6 mm OD x 1/8 in. Male NPT 2 x tube fitting, Swagelok PFA 1/8 in. OD x 1/8 in. Male NPT 1 x T probe fitting, modified Swagelok PFA 3 mm OD x 1/8 in. Male NPT 1 x Swagelok PFA plug for tube size 1/8 in. OD (if T probe not used) 1 x Swagelok PFA plug for tube size 6 mm OD (for 2-electrode setup) 1 x O-ring, FKM 1 x PTFE tape Related products High-pressure working electrode High-pressure counter electrode High-pressure reference electrode High-pressure basic sampel holder